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Pengaruh Suhu Kalsinasi pada Proses Dekomposisi Dolomit

机译:煅烧温度对白云石分解过程的影响

摘要

THE EFFECT OF CALCINATION TEMPERATURE ON THE DECOMPOSITION OF DOLOMITE. Decomposition of dolomite to MgO and CaO is important because both these oxides are widely used in various applications. To determine the effect of calcination temperature on the decomposition of dolomite to MgO and CaO, the calcination was investigated. The Muffle furnace was used to calcination process at temperatures of 500, 600, 700, 800 and 900 oC. A total of dolomite (100 gram) was put in a furnace and heated with a heating rate of 10 oC /min at various temperatures and then arrested with holding time 1, 2, 3, 4 and 5 hours, respectively. The calcined samples were then weight measured and characterized by X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM). The experimental results indicated that the decomposition of dolomite increases with the increases of the calcination temperature. The optimum calcination conditions are achieved at 900 °C for 4 hours. Under the optimum conditions, the weight loss of dolomite can reach 46.74%. Based on stoichiometry calculations 46.74% weight reduction showed that 97.78% of dolomite decomposed into MgO and CaO. The decomposition of dolomite into CaO and MgO through two stages, namely stages of formation of MgO-CaCO3 at 700 oC and CaO at 800 °C - 900 °C. The conclusions obtained from this calcination of dolomite is the raising of calcination temperature can improve the process of decomposition of dolomite into MgO and CaO.
机译:煅烧温度对白云石分解的影响。将白云石分解为MgO和CaO很重要,因为这两种氧化物都广泛用于各种应用中。为了确定煅烧温度对白云石分解为MgO和CaO的影响,对煅烧进行了研究。马弗炉用于在500、600、700、800和900 oC的温度下进行煅烧。将总计为100克的白云石放入炉中,并在各种温度下以10 oC / min的加热速率进行加热,然后在保持时间分别为1、2、3、4和5小时的条件下停止。然后测量煅烧样品的重量,并通过X射线衍射(XRD)和扫描电子显微镜(SEM)表征。实验结果表明,随着煅烧温度的升高,白云石的分解增加。最佳煅烧条件是在900°C下保持4小时。在最佳条件下,白云石的失重可达到46.74%。根据化学计量计算,重量减少46.74%,表明97.78%的白云石分解为MgO和CaO。白云石通过两个阶段分解为CaO和MgO,即在700 oC形成MgO-CaCO3和在800°C-900°C形成CaO的阶段。从白云石的煅烧中得出的结论是,提高煅烧温度可以改善白云石分解为MgO和CaO的过程。

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